$Version: 4 $Totobjs: 13 $Pen_RGB2Color: 0 0 0 $Fill_RGB2Color: 0 0 0 $Font: "Times New Roman" 120 0 $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 1990 1017 3960 1204 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f3720\nil Times New Roman;} {\f3468\nil Times New Roman;} } \plain \f3720\fs24 (i) 2 SiPh \plain \f3468\fs24\dn6 2 \plain \f3720\fs24 Cl \plain \f3468\fs24\dn6 2 \plain \f3720\fs24 , thf, 4 h, hexane extraction } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 2005 807 3188 972 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f1268\nil Times New Roman;} } \plain \f1268\fs24 Reagents and conditions } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 553 483 1152 648 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f1344\nil Times New Roman;} {\f3464\nil Times New Roman;} } \plain \f1344\fs24 2 LiC \plain \f3464\fs24\dn6 5 \plain \f1344\fs24 HMe \plain \f3464\fs24\dn6 4 } $Obj: line $ArrowDir: 1 $ArrowStyle: 1 $ArrowSize: 57 64 cm cm $RxnAtch: -1 -1 $Obj_coords: 1206 562 1611 562 $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 1325 385 1437 527 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f1752\nil Times New Roman;} {\f1652\nil Times New Roman;} } \plain \f1652\fs24 (i) } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 1617 475 2726 647 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f1168\nil Times New Roman;} {\f912\nil Symbol;} {\f3848\nil Times New Roman;} {\f1696\nil Times New Roman;} } \plain \f1168\fs24 2 Si( \plain \f912\fs24 h \plain \f3848\fs24\up6 1 \plain \f1168\fs24 -C \plain \f1696\fs24\dn6 5 \plain \f1168\fs24 HMe \plain \f1696\fs24\dn6 4 \plain \f1168\fs24 )Ph \plain \f1696\fs24\dn6 2 \plain \f1168\fs24 Cl } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 1292 607 1547 749 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f1724\nil Times New Roman;} {\f2036\nil Times New Roman;} } \plain \f2036\fs24 97 % } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 2793 597 3048 739 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f924\nil Times New Roman;} } \plain \f924\fs24 70 % } $Obj: line $ArrowDir: 1 $ArrowStyle: 1 $ArrowSize: 57 64 cm cm $RxnAtch: -1 -1 $Obj_coords: 2741 555 3135 559 $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 3186 465 4429 637 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f1912\nil Times New Roman;} {\f1472\nil Symbol;} {\f404\nil Times New Roman;} } \plain \f1912\fs24 [Fe\{ \plain \f1472\fs24 h \plain \f1912\fs24 -C \plain \f404\fs24\dn6 5 \plain \f1912\fs24 Me \plain \f404\fs24\dn6 4 \plain \f1912\fs24 (SiPh \plain \f404\fs24\dn6 2 \plain \f1912\fs24 Cl)\} \plain \f404\fs24\dn6 2 \plain \f1912\fs24 ] } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 1994 1222 4398 1544 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f1952\nil Times New Roman;} {\f1624\nil Times New Roman;} {\f2832\nil Times New Roman;} } \plain \f1952\fs24 (ii) 2 LiBu \plain \f1624\fs24\up6 t \plain \f1952\fs24 , thf, -78 \plain \f1624\fs24\up6 o \plain \f1952\fs24 C, FeCl \plain \f2832\fs24\dn6 2 \plain \f1952\fs24 , hexane wash, Et \plain \f2832\fs24\dn6 2 \plain \f1952\fs24 O \plain \f1952\fs24 \par \plain \f1952\fs24 extraction. Recrystallisation from hot toluene } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 3672 675 3754 817 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f1892\nil Times New Roman;} {\f4012\nil Times New Roman;} } \plain \f4012\fs24\b 2 } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 2839 379 2981 521 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f1444\nil Times New Roman;} {\f3960\nil Times New Roman;} } \plain \f3960\fs24 (ii) } $Endsketch: