$Version: 4 $Totobjs: 14 $Pen_RGB2Color: 0 0 0 $Fill_RGB2Color: 0 0 0 $Font: "Times New Roman" 120 0 $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 1314 582 1426 724 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f3452\nil Times New Roman;} } \plain \f3452\fs24 (i) } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 1633 1384 4090 1549 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f2000\nil Times New Roman;} {\f2456\nil Times New Roman;} {\f1736\nil Times New Roman;} } \plain \f2000\fs24 (i) Et \plain \f2456\fs24\dn6 2 \plain \f2000\fs24 O, -78 \plain \f1736\fs24\up6 o \plain \f2000\fs24 C, 2 SiMe \plain \f2456\fs24\dn6 2 \plain \f2000\fs24 (NEt \plain \f2456\fs24\dn6 2 \plain \f2000\fs24 )Cl, 12 h, distillation } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 1641 1175 2809 1317 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f1372\nil Times New Roman;} } \plain \f1372\fs24 Reagents and conditions } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 1640 670 2973 842 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f3604\nil Times New Roman;} {\f2408\nil Symbol;} {\f796\nil Times New Roman;} } \plain \f3604\fs24 Fe[ \plain \f2408\fs24 h \plain \f3604\fs24 -C \plain \f796\fs24\dn6 5 \plain \f3604\fs24 H \plain \f796\fs24\dn6 4 \plain \f3604\fs24 \{SiMe \plain \f796\fs24\dn6 2 \plain \f3604\fs24 (NEt \plain \f796\fs24\dn6 2 \plain \f3604\fs24 )\}] \plain \f796\fs24\dn6 2 } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 3097 575 3239 717 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f3744\nil Times New Roman;} {\f2800\nil Times New Roman;} } \plain \f2800\fs24 (ii) } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 173 670 1199 842 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f2028\nil Times New Roman;} {\f2848\nil Symbol;} {\f1280\nil Times New Roman;} } \plain \f2028\fs24 Fe( \plain \f2848\fs24 h \plain \f2028\fs24 -C \plain \f1280\fs24\dn6 5 \plain \f2028\fs24 H \plain \f1280\fs24\dn6 4 \plain \f2028\fs24 Li.tmeda) \plain \f1280\fs24\dn6 2 } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 3401 678 4525 850 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f928\nil Times New Roman;} {\f3064\nil Times New Roman;} {\f2048\nil Symbol;} } \plain \f3064\fs24 Fe\{ \plain \f2048\fs24 h \plain \f3064\fs24 -C \plain \f928\fs24\dn6 5 \plain \f3064\fs24 H \plain \f928\fs24\dn6 4 \plain \f3064\fs24 (SiMe \plain \f928\fs24\dn6 2 \plain \f3064\fs24 Cl)\} \plain \f928\fs24\dn6 2 } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 1626 1593 3663 1758 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f2144\nil Times New Roman;} {\f508\nil Times New Roman;} {\f2132\nil Times New Roman;} } \plain \f508\fs24 (ii) Et \plain \f2144\fs24\dn6 2 \plain \f508\fs24 O, 0 \plain \f2132\fs24\up6 o \plain \f508\fs24 C, 2 MeCOCl, 3 h, distillation } $Obj: line $ArrowDir: 1 $ArrowStyle: 1 $ArrowSize: 57 64 cm cm $RxnAtch: -1 -1 $Obj_coords: 1242 763 1572 763 $Obj: line $ArrowDir: 1 $ArrowStyle: 1 $ArrowSize: 57 64 cm cm $RxnAtch: -1 -1 $Obj_coords: 3025 763 3355 763 $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 1277 806 1532 948 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f1552\nil Times New Roman;} } \plain \f1552\fs24 59 % } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 3076 798 3331 940 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f2060\nil Times New Roman;} } \plain \f2060\fs24 82 % } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 2026 926 2483 1068 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f1980\nil Times New Roman;} } \plain \f1980\fs24 red liquid } $Obj: text $Transparent: $RxnAtch: -1 -1 $Obj_coords: 3517 919 4461 1061 $MDLEdittext: 1 000b {\rtf1\defformat\pc {\fonttbl {\f2088\nil Times New Roman;} } \plain \f2088\fs24 yellow-orange solid } $Endsketch: